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PPM Fluid - what's best?

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  • PPM Fluid - what's best?

    Have done some reading about ppm fluids. Seems most use
    water or an alcohol (ethanol, methanol).
    If I understand (please correct me as needed ) the ppm
    detects the protons in hydrogen as they spin out of
    alignment.
    So it seems that if the fluid has relatively more H it will
    generate a stronger signal. With this in mind, I spent a few
    minutes with wikipedia and a spreadsheet (OpenOfficeCalc)
    and found the following:

    Code:
    Substance      Formula       Density          %H
    Water        H2O               1.00          100.0
    Propane      C3H8              0.58           95.4
    Butane       C4H10             0.60           92.9
    Methanol     CH4O              0.79           88.4
    Ethanol      C2H6O             0.79           92.2
    Paraffin     C25H52            0.93          123.6


    Six "fluids" are listed with their formulas, densities, and % of
    H relative to water. I used molecular weights and grams/mol
    to derive the result.
    So, given the potential for a 20% gain in signal strength,
    has anyone used paraffin (wax) as a working fluid? If not,
    why? It seems that because it is "solid" at room temps
    it would be quite easy to work with.

    regards,

    thom

  • #2
    It MUST be liquid

    to work...

    Comment


    • #3
      Aha... thank you. I knew there must be a reason.
      I'll keep reading and learning.

      regards,

      thom

      Comment


      • #4
        PPM Fluid-what's best?

        Not a problem-liquid paraffin is also known as Mineral Oil.

        From Wikipedia:

        Mineral oil

        Main article: Mineral oil
        Liquid paraffin, or mineral oil, is a mixture of heavier alkanes, and has a number of names, including nujol, adepsine oil, alboline, glymol, medicinal paraffin, or saxol. It has a density of around 0.8 g/cm3.


        Randy

        Comment


        • #5
          Some proton magnetometers used Kerosene. I believe it gives a faster proton alignment.

          Liquid paraffin may be similar.

          Tinkerer

          Comment


          • #6
            Pure Liqued paraffin wax

            Here is true liquid 100% paraffin wax:

            http://www.instawares.com/soft-light-disposable-liquid.977076.0.7.htm?gclid=CPLD6fnOqKMCFQUbawodRC sH4A&s_kwcid=TC|20025|liquid paraffin wax||S|p|5839841289&

            Used for candles. Paraffin is what Purcell,Pound and Torrey used in their discovery of nuclear magnetic resonance,for which they won the Nobel Prize (from pg.12 of the book "Signals from the Subatomic World" by Stefan Hollos and Richard Hollos-200.

            Randy

            Comment


            • #7
              Tried editing 3 times

              Should read 2008 for the copyright. Tried saving my corrections three times and goes back to the happy face,oh well.

              Randy

              Comment


              • #8
                Originally posted by Seden View Post
                Should read 2008 for the copyright. Tried saving my corrections three times and goes back to the happy face,oh well.

                Randy
                This happens when you type an "8" followed by ")". For example: (200
                The solution is to type ( 2008 ).

                Comment


                • #9
                  Originally posted by Tinkerer View Post
                  Some proton magnetometers used Kerosene. I believe it gives a faster proton alignment.

                  Liquid paraffin may be similar.

                  Tinkerer

                  We are using isopropyl alcohol (isopropylene). This is the alcohol used to clean the white boards and the TV and PC Screens. It is widely available and cheap. We get very good signals from a polarization duration as small as 600msec which gives us a practical reading rate of one per second.
                  I have also used the type of alcohol used to light the BBQ,thaty works almost as well. The problem with kerosene is that it is a mixture of undefined percentages of many simple components and that could give very different results from one sample to the other. It also smells very bad!!!
                  Willy

                  Comment


                  • #10
                    PPM fluid additives?

                    Originally posted by ToyMaker View Post
                    Have done some reading about ppm fluids. Seems most use
                    water or an alcohol (ethanol, methanol).
                    If I understand (please correct me as needed ) the ppm
                    detects the protons in hydrogen as they spin out of
                    alignment.
                    So it seems that if the fluid has relatively more H it will
                    generate a stronger signal. With this in mind, I spent a few
                    minutes with wikipedia and a spreadsheet (OpenOfficeCalc)
                    and found the following:

                    Code:
                    Substance      Formula       Density          %H
                    Water        H2O               1.00          100.0
                    Propane      C3H8              0.58           95.4
                    Butane       C4H10             0.60           92.9
                    Methanol     CH4O              0.79           88.4
                    Ethanol      C2H6O             0.79           92.2
                    Paraffin     C25H52            0.93          123.6


                    Six "fluids" are listed with their formulas, densities, and % of
                    H relative to water. I used molecular weights and grams/mol
                    to derive the result.
                    So, given the potential for a 20% gain in signal strength,
                    has anyone used paraffin (wax) as a working fluid? If not,
                    why? It seems that because it is "solid" at room temps
                    it would be quite easy to work with.

                    regards,

                    thom
                    I've read that the commercial manufactures have proprietary additives to make
                    the fluids work better. One idea is to use distilled water and add an 'ion' additive.
                    This I surmise helps couple the first RF pulse to the fluid which can then couple this energy to the magnetic domain for subsequent steps. I think this might be an
                    acid of some kind.

                    Comment


                    • #11
                      Originally posted by bmoore View Post
                      This I surmise helps couple the first RF pulse to the fluid which can then couple this energy to the magnetic domain for subsequent steps.
                      Are we still talking about proton precession mags???

                      Comment


                      • #12
                        Originally posted by Boattow View Post
                        Are we still talking about proton precession mags???
                        No, this is the principle used in Overhauser systems but it also needs an RF excitation coil.

                        Willy

                        Comment


                        • #13
                          Originally posted by Willy Bayot View Post
                          We are using isopropyl alcohol (isopropylene). This is the alcohol used to clean the white boards and the TV and PC Screens. It is widely available and cheap. We get very good signals from a polarization duration as small as 600msec which gives us a practical reading rate of one per second.
                          I have also used the type of alcohol used to light the BBQ,thaty works almost as well. The problem with kerosene is that it is a mixture of undefined percentages of many simple components and that could give very different results from one sample to the other. It also smells very bad!!!
                          Willy
                          Today, I first tested isopropyl alcohol (isopropylene) in the proton magnetometer PPMA-3. Large improvements in the device compared to kerosene had not noticed. The device works fine when the polarization of 600 ms. Boundary of stable operation - 400 ms

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